cond-mat.mtrl-sciAug 19, 2026

Multi-Tool Robotics Enables In-Situ Sample Manipulation for Time-Resolved Synchrotron Measurements

Authors: Aditya Bondada, Elizabeth M. Wall, Eric Yuan Xiao, Quinn C. Burlingame, Yueh-Lin Loo, Esther H. R. Tsai, Ruipeng Li

Organizations: Center for Functional Nanomaterials Brookhaven National Laboratory Upton, NY 11973, USA · Department of Chemical and Biological Engineering Princeton University Princeton, NJ 08540, USA · Department of Mechanical Engineering Stony Brook University Stony Brook, NY 11790, USA · National Synchrotron Light Source II Brookhaven National Laboratory Upton, NY 11973, USA

Abstract

The high photon flux at synchrotron beamlines allows for the measurement of fast dynamical processes. However, beamline radiation-safety protocols prohibit human intervention during X-ray experiments, limiting the ability to perform versatile real-time sample manipulations during continuous data acquisition. Here we present a robotic platform at an X-ray scattering beamline to enable real-time sample handling and processing in the experimental hutch, revealing previously inaccessible transient in-situ dynamics in perovskite thin films. This modular multi-tool robotic architecture enables in-hutch sample manipulation beyond human-access constraints, establishing a foundation for automated and autonomous synchrotron experimentation.

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